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Week
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Topics
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Study Metarials
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1
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Rules and general information to be followed in the laboratory(introduction of laboratory materials, safety of chemicals, report preparation)
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R1 CHAPTER 1
R2 CHAPTER 1
R3 CHAPTER A 1.2 and 1.3
SB1 CHAPTER 1 and 2
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2
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Introduction of distillation varieties and separation of liquid components through simple and fractional
distillation.
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R1 CHAPTER 1
R2 CHAPTER 2 and 3
R3 CHAPTER A 1.2 and 1.3
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3
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Extraction, Recrystallization
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R1 CHAPTER 1
R2 CHAPTER 2
R3 CHAPTER A 2.1 and 2.5
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4
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Isolation of Caffeine from Tea / Determination of Melting Point
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R1 CHAPTER 1
R3 CHAPTER A 3.1 and 6.11
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5
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Synthesis of o,p-Nitrophenol
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R2 CHAPTER 2
R3 CHAPTER 1.7
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6
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Chromatography (introduction of Column Chromatography and TLC (Thin layer chromatography) and purification of o, p-nitro phenol through column chromatography)
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R1 CHAPTER 1
R3 CHAPTER A 2.7 and 2.9
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7
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Synthesis of Cyclohexene and unsaturation test
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R1 CHAPTER 2
R3 CHAPTER B 1.2.1
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8
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Sublimation
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R1 CHAPTER 1
R3 CHAPTER A 2.4
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9
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Synthesis of Phenyl Azo-beta-naphthol
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R1 CHAPTER 2
R3 CHAPTER B 1.22.3 and 4.1
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10
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Synthesis of Acetylsalicylic Acid (Aspirin)
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R1 CHAPTER 2
R2 CHAPTER 3
R3 CHAPTER B 1.13 and 3.1
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11
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Condensation reactions (Synthesis of benzalacetone) and iodoform test.
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R1 CHAPTER 2
R3 CHAPTER B 1.11.27
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12
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FTIR spectroscopy (interpretation of aspirin, benzalacetone and phenyl Azo-beta-naphthol by taking IR spectrum)
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R3 CHAPTER D, 3
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13
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NMR spectroscopy (interpretation of aspirin by taking 1-H and 13-C)
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R3 CHAPTER D, 4
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14
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Mass (GC-MS) introduction and analysis of organic molecules
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R3 CHAPTER D, 5
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Prerequisites
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-
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Language of Instruction
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Turkish
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Responsible
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Prof. Dr. Zeynep GÜLTEKİN
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Instructors
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-
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Assistants
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Dr. Serkan KOLDAŞ, Dr. Ali Rıza TÜFEKÇİ
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Resources
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R1. Hocaoğlu, N.; Uyar T. 1990. Organik Kimya Laboratuarı.
R2. Gülten Ş. 2006. Genel Kimya Laboratuarı ISBN: 975-295-576-2
R3. Erdik, E.; Obalı M.; Yüksekışık,N.; Öktemer, A.; Pekel,T. 2013. Denel Organik Kimya. (7. Baskı),
ISBN: 978-975-6009-93-2
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Supplementary Book
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SB1. Güler, K.; Saraydın, D.; Ulusoy U. 2006 (6. Baskı). Genel Kimya Laboratuarı,
ISBN: 975 7527-74-2
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Goals
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The aim of this course is to teach the students the rules and safety of working in the laboratory, as well as to teach the basic laboratory methods of synthesis, purification of organic molecules and spectroscopic recognition of these compounds.
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Content
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Rules to be followed in the laboratory, introduction of distillation varieties.
Extraction, crystallization, melting point determination. Isolation of caffeine from tea. Synthesis of o,p-nitrofenol, cyclohexene, phenyl azo-beta-naphthol , acetylsalicylic acid and benzalacetone. Chromatography (column chromatography and definition of TLC), introduction of FTIR and NMR spectroscopy instruments and characterization of organic molecules
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Program Learning Outcomes |
Level of Contribution |
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1
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Has the necessary theoretical and applied basic knowledge in the basic fields of chemistry.
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-
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2
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Designs experiments and develops solution methods for research and problems related to chemistry, solve problems using appropriate analytical methods and techniques, collects data, and analyzes and interprets the results.
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4
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3
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Has the ability to use library facilities, written and online information resources to access up-to-date theoretical and practical information about chemistry.
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3
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4
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Follows the current developments in the field of science and technology, improves their knowledge, conducts an examination using scientific methods and techniques, and independently conducts advanced work related to their field.
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-
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5
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Participates in interdisciplinary studies by using basic knowledge and analytical thinking ability.
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3
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6
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Adapts theoretical and practical information to conditions to develop realistic solutions and strategies in scientific terms.
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4
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7
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Plans and manages activities for the professional development of employees in the chemical-related sectors under his responsibility.
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-
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8
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Takes responsibility for lifelong learning and teaching, follows current developments in chemistry and related fields, and constantly renews itself.
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-
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9
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Has a level of foreign language knowledge that will be able to access the scientific information needs from foreign sources related to his field, update knowledge, and communicate with colleagues around the world.
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-
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10
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Uses information and communication technologies along with computer software at the level required by the field for molecular modeling and chemical calculations.
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-
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11
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Informs the relevant persons and institutions on chemistry-related issues, and expresses his thoughts, and suggestions for solutions to problems, using effective written or oral communication in Turkish.
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-
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12
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Uses knowledge about the field of chemistry in the profession and daily life with the awareness of social responsibility.
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-
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13
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Has awareness of scientific and social rules and cultural and ethical values to carry out teamwork effectively and safely, as well as the technical rules that must be followed while conducting studies in its field.
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-
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14
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Uses related knowledge on human health and environmental consciousness for the benefit of the society.
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4
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